Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion

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	Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion
	D. Y. Han; H. Y. Yang; C. B. Shen; X. Zhou; F. H. Wang
	2004
发表期刊	Powder Technology
ISSN	0032-5910
卷号	147 期号:1-3 页码:113-116
摘要	Nanoparticles of NiO were successfully prepared by Triton X-100/n-hextnol/cyclohexane/water W/O microemulsion system. Basic synthesis parameters were determined. The result of TG-DTA analysis of the precursor products showed that the proper calcination temperature was 450 degreesC. The nanoparticles were characterized by X-ray diffractometer (XRD), transmission electron microscopy (TEM) and UV-VIS spectra. The results showed that the nanoparticle was exactly NiO with cubic rock salt structure and the size of nanoparticles was strongly affected by the ratio of water to surfactant (R) and also the calcined temperature. With the R value increased, the particles size became larger; with the calcined temperature increased, the particles size also became larger. (C) 2004 Elsevier B.V. All rights reserved.
部门归属	chinese acad sci, inst met res, state key lab corros & protect, shenyang 110016, peoples r china. dalian inst railway technol, dept mat sci & engn, dalian 116028, peoples r china.;han, dy (reprint author), chinese acad sci, inst met res, state key lab corros & protect, shenyang 110016, peoples r china;dyhan@imr.ac.cn
关键词	Microemulsion Nio Nanoparticles Synthesis Particles
URL	查看原文
WOS记录号	WOS:000225808900011
引用统计	被引频次：113[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/35367
专题	中国科学院金属研究所
推荐引用方式 GB/T 7714	D. Y. Han,H. Y. Yang,C. B. Shen,et al. Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion[J]. Powder Technology,2004,147(1-3):113-116.
APA	D. Y. Han,H. Y. Yang,C. B. Shen,X. Zhou,&F. H. Wang.(2004).Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion.Powder Technology,147(1-3),113-116.
MLA	D. Y. Han,et al."Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion".Powder Technology 147.1-3(2004):113-116.