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Preparation and characterization of polystyrene microcapsules containing liquid polysulfide rubber
Wang, Xuan1,2; Yuan, Xuwen1,2,3; Fan, Shuimei1; Yang, Huaiyu1,2
通讯作者Yuan, Xuwen(20210015@huat.edu.cn) ; Yang, Huaiyu(hyyang@imr.ac.cn)
2024-09-20
发表期刊COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS
ISSN0927-7757
卷号697页码:10
摘要In this paper, the microcapsules containing liquid polysulfide rubber (LPR) are firstly prepared by solvent evaporation method with dichloromethane (DCM) as solvent and polystyrene (PS) as shell material. The effects of surfactant type and dosage, stirring rate, core-shell mass ratio and oil/water phase volume ratio on the encapsulation effect of LPR are investigated to obtain the following optimized preparation condition: using 4 wt % NaOA solution as the dispersed phase, DCM as the volatile organic solvent, stirring rate of 500 rpm as the preparation conditions, the obtained microcapsules are spherical and smooth, the average particle size is 30.01 mu m, the ratio of oil phase to water phase is 1:6, and the core-shell mass ratio is 0.8:1. The content of LPR in microcapsules is 43 %, which is calculated according to the thermogravimetric analysis (TGA) curve. The research results provide an important theoretical basis and technical support for promoting the engineering application of viscous fluid materials represented by LPR.
关键词Liquid polysulfide rubber Solvent evaporation method Polystyrene Microcapsules
资助者Ministry of Industry and Information Technology ; Hubei Provincial Natural Science Foundation of China ; PhD Research Startup Foundation of Hubei Univer- sity of Automotive Technology
DOI10.1016/j.colsurfa.2024.134410
收录类别SCI
语种英语
资助项目Ministry of Industry and Information Technology[MJ- 2014-F-14] ; Hubei Provincial Natural Science Foundation of China[2022CFB922] ; PhD Research Startup Foundation of Hubei Univer- sity of Automotive Technology[BK202103]
WOS研究方向Chemistry
WOS类目Chemistry, Physical
WOS记录号WOS:001249490200001
出版者ELSEVIER
引用统计
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/187340
专题中国科学院金属研究所
通讯作者Yuan, Xuwen; Yang, Huaiyu
作者单位1.Chinese Acad Sci, Inst Met Res, Shenyang 110016, Peoples R China
2.Univ Sci & Technol China, Sch Mat Sci & Engn, Hefei 230026, Peoples R China
3.Hubei Univ Automot Technol, Dept Mat Sci & Engn, Shiyan 442002, Peoples R China
推荐引用方式
GB/T 7714
Wang, Xuan,Yuan, Xuwen,Fan, Shuimei,et al. Preparation and characterization of polystyrene microcapsules containing liquid polysulfide rubber[J]. COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS,2024,697:10.
APA Wang, Xuan,Yuan, Xuwen,Fan, Shuimei,&Yang, Huaiyu.(2024).Preparation and characterization of polystyrene microcapsules containing liquid polysulfide rubber.COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS,697,10.
MLA Wang, Xuan,et al."Preparation and characterization of polystyrene microcapsules containing liquid polysulfide rubber".COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS 697(2024):10.
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